Lithium-Ion Batteries Recycling

Lithium-ion Battery Recycling

 

Introduction and uses:

Lithium-ion batteries are amongst the most commonly used in the world, with the usage varying from handheld small electronic devices such as electronics, toys, wireless headphones to electric cars and energy storage systems we use today. These batteries are greatly preferred due to their high energy density, i.e. the ability to store energy efficiently in a given amount of space. Lithium batteries are smaller and lighter than other types of batteries, and have a greater energy density, leading to its greater use compared to other kinds of batteries. Lithium cells are of two types- one made of lithium metal which are single use and non-rechargeable, and the other which are made out of lithium and polymer and are multi use and non-rechargeable.

 

Structure of a li-ion battery:

A lithium-ion battery comprises of a cathode, an anode and an electrolyte. The anode is usually made of carbon(graphite), the cathode of a metal oxide (such as lithium cobalt oxide, lithium manganese oxide) and the electrolyte usually being lithium salt in an organic solvent. The anode and cathode do not short due to a separator, and their electrochemical roles reverse depending on the direction of flow of current through the cell.

When in use, during discharge, the lithium ions are which stored in a mesh of the graphite anode, travel through the electrolyte, while the electrons travel through the external circuit, powering it; and the two recombine at the cathode. Thus, an oxidation half reaction takes place at the anode while a reduction half reaction takes place at the cathode.

During charging, the reverse process takes place, with the electrons travelling from the cathode to the anode from the external circuit and the lithium ions move across the electrolyte towards the anode.

 

Future Problems:

Lithium ion batteries often contain many such important metals like cobalt, nickel, manganese, which are necessary and are considered as critical minerals, due to their strategic and economical importance, with their supply being at high risk due to problems in the supply chain and no easy substitutes being available. Outright disposal of these batteries leads to loss of these recoverable minerals, as well as posing a health and fire hazard if not disposed properly.

In the past few years, with over 1,80,000 metric tons of Li-ion batteries being available worldwide for recycling, a little over half were recycled. Thus, there is a need for recycling of these batteries in order to prevent excessive mining for these minerals, saving the environment and thereby lies an opportunity for recycling of these batteries.

Process:

Recycling of these batteries begins with separating them and to sort them by the type of battery, as each type of chemical make-up requires its own process. Most of the recycling of these batteries occurs in one of these paths:

1.     1Direct method: Here, the battery is disassembled, and the cathode is separated, as it needs the reconditioning. A lithium source is then added, in order to replenish the used cathode, which is then followed by the process of calcination. This method is the most widely used, as it allows recyclers to keep the crystal structure intact with lower energy, reagents and fixed facility costs, while having a smaller impact on the environment than hydrometallurgy and pyrometallurgy. It has a short recovery route and is environmentally friendly, along with having a high recovery rate and low energy consumption. However, it has high operational and equipment requirements and incomplete recovery.

2.    2.  Pyrometallurgy: This method is most used when there exist rare earth minerals such as cobalt, etc which need to be recycled. In reductive smelting, after pre-treatment, battery materials are heated under vacuum or inert atmosphere to convert metal oxides to metal alloy containing cobalt, nickel, iron, slag containing lithium and aluminium. This is also accompanied by the emission of greenhouse gases.  The pre-treatment methods often are crushing and shredding. The end product is the recovered metal allow which can be further processed and used according to requirements. IT is a highly efficient process with simple operation and short flow. However, energy consumption is high, with waste gas being formed and low efficiency of recovery rate.

3.   3.   Hydrometallurgy: Hydrometallurgical methods use primarily aqueous solutions to extract and separate metals from the batteries. The pre-treated battery materials (with aluminium and copper parts removed) are most often extracted with H2SO4 and H2O2, although HCl, HNO3, and organic acids including citric and oxalic acids are commonly used. Once metals have been extracted into solution, they are precipitated selectively as salts using pH variation or extracted using organic solvents containing extractants such as dialkyl phosphates or phosphinates. The advantages of this process being that the recovery rate and product purity is high, with energy consumption and waste gas emission being low. However, it is a long process with ample wastewater being formed.

 

In many cases, we see that pyrometallurgy and hydrometallurgy is often used together.

 



 

Economic Outlook:

A 2022 report from McKinsey says that the entire Li-ion battery chain, from mining to recycling could grow over 30% in value, reaching a value of $400 billion and a market size of 4.7 TWh. With governmental norms in place and an overall push for more reusing and recycling, along with the unstable supply chain for various metals required in batteries such as nickel and cobalt, it is essential to develop recycling of lithium-ion batteries on a large scale in order, as the future requirements are incredibly demanding and vital. By 2040, the recycling industry alone could generate revenues of over $40 billion and have a profit pool of $6 billion.

 

 

By Vedant Banthia (Tech Tuesday, COEP BLOGS)

 Credits and References:

1.     Lithium-Ion Battery Recycling & Overview of Techniques and Trends

2.     https://www.mckinsey.com/industries/automotive-and-assembly/our-insights/battery-2030-resilient-sustainable-and-circular

3.     https://www.epa.gov/recycle/used-lithium-ion-batteries

4.     https://spectrum.ieee.org/lithiumion-battery-recycling-finally-takes-off-in-north-america-and-europe

 


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